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  • ao.chen@setaram.cn
  • Room 509, Building A, Block 3, No.128 Huayuan Rd, Shanghai,CHINA

PRODUCTS

Thermogravimetric Analyzer(setline TGA)

Simple & Powerful

Setline TGA can measure the quality change process of samples in real time under the conditions of specific atmosphere and program temperature control, so as to obtain the weight loss information such as dehydration, decomposition, desorption, volatilization or weight gain information such as hydration, oxidation, adsorption.


High precision photoelectric balance

 

 

APPLICATIONS

Adsorption Corrosion/Oxidation  Decomposition
Reactions
Dehydration Desolvation Desorption
Evaporation Mass change Residual mass
Solid-gas reaction Thermogravimetric
analysis
Volatiles
determination

 

PARAMETERS

Temperature  range RT~1100°C
Programmable heating rate 0.01~50°C/min
Temperature accuracy ±0.1°C
Mass variation resolution 0.02ug
baseline drift <10ug(1hour)
Mass variation range ±1000mg

For more information, please click on the website(http://www.setaram.cn

APPLICATIONS

Calcium oxalate monohydrate (CaC2O4,H2O) samples were measured by mass loss (TG) and heat flow (DSC). From lower temperature to higher temperature: dehydration, formation of calcium carbonate and formation of calcium oxide. This simple case highlights the application of thermogravimetric analysis in quantitative measurement.

Analysis of synthetic rubber components. 
The sample was heated to 600°C in two steps under an inert atmosphere (N2) and then cooled to 400°C, and the atmosphere was switched to air, the sample was heated to 800°C after holding for a period of time. The TG curve has three mass losses corresponding to the decomposition of plasticizers: oil and wax content (3.6%), elastomer content (57.9%) and carbon black content (38.7%). The remaining mass at the end of the experiment corresponds to the ash content of the rubber (<0.5%).

 

ASTM Number Title Website Link
E1582-14 Standard Practice for Calibration of Temperature Scale for Thermogravimetry Link
E2040-08 Standard Test Method for Mass Scale Calibration of Thermogravimetric Analyzers Link
E2402-11 Standard Test Method for Mass Loss and Residue Measurement Validation of Thermogravimetric Analyzers Link
E1131-08 Standard Test Method for Compositional Analysis by Thermogravimetry Link
D6370-99 Standard Test Method for Rubber–Compositional Analysis by Thermogravimetry (TGA) Link
E1868-10 Standard Test Methods for Loss-On-Drying by Thermogravimetry Link
E2008-08e1 Standard Test Methods for Volatility Rate by Thermogravimetry Link
E2550-11 Standard Test Method for Thermal Stability by Thermogravimetry Link
D6382-99 Standard Practice for Dynamic Mechanical Analysis and Thermogravimetry of Roofing and Waterproofing Membrane Material Link
E1877-15 Standard Practice for Calculating Thermal Endurance of Materials from Thermogravimetric Decomposition Data Link
E2403-06 Standard Test Method for Sulfated Ash of Organic Materials by Thermogravimetry Link
E2043-99 Standard Test Method for Nonvolatile Matter of Agricultural Adjuvant Solutions by Thermogravimetry Link
D3850-12 Standard Test Method for Rapid Thermal Degradation of Solid Electrical Insulation Materials By Thermogravimetric Method (TGA) Link

 

ISO Number Title Website Link
11358 Plastics– Thermogravimetry (TG) of polymers Link
9924 Rubber and rubber products– Determination of the composition of vulcanizates and uncured compounds by thermogravimetry Link
21870 Rubber compounding ingredients– Carbon black– Determination of high-temperature loss on heating by thermogravimetry Link
11308 Nanotechnologies– Characterization of single-wall carbon nanotubes using thermogravimetric analysis Link