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PRODUCTS

Simultaneous thermal analysis (setline STA)

Simple & Powerful

Simultaneous thermal analysis (STA) is the combination of thermogravimetric analysis (TGA) and differential thermal analysis (DTA) or differential scanning calorimetry (DSC). The mass change and heat flow change can be obtained once measurement on one instrument. 

APPLICATIONS

Adsorption Catalytic reaction Compositional analysis
Corrosion/Oxidation Crystallization Curing
Decomposition Differential scanning calorimetry Evaporation
Glass transition temperature Magnetic transitions Mass change
Phase diagram Phase transition temperature Purity determination
Reaction kinetics Residual mass Simultaneous thermal analysis
Solid-gas reactions Solid-liquid reactions Solid-solid reaction
Specific heat determination Sublimation Synthesis reactions
Thermal stability Thermogravimetric analysis Transition enthalpies

 

PARAMETERS

Temperature  range RT~1100°C
Programmable heating rate 0.01~50°C/min
Temperature precision ±0.05°C
 Mass variation resolution 0.02ug
 Mass variation range  ±1000mg
Autosampler 51(sample and reference )

For more information, please click on the website(http://www.setaram.cn

APPLICATIONS

Calcium oxalate monohydrate (CaC2O4,H2O) samples were measured by mass loss (TG) and heat flow (DSC). From lower temperature to higher temperature: dehydration, formation of calcium carbonate and formation of calcium oxide. This simple case highlights the application of thermogravimetric analysis in quantitative measurement.

Analysis of synthetic rubber components. 
The sample was heated to 600°C in two steps under an inert atmosphere (N2) and then cooled to 400°C, and the atmosphere was switched to air, the sample was heated to 800°C after holding for a period of time. The TG curve has three mass losses corresponding to the decomposition of plasticizers: oil and wax content (3.6%), elastomer content (57.9%) and carbon black content (38.7%). The remaining mass at the end of the experiment corresponds to the ash content of the rubber (<0.5%).

ASTM Number Title Website Link
E968-02 Standard Practice for Heat Flow Calibration of Differential Scanning Calorimeters Link
E2253-11 Standard Test Method for Temperature and Enthalpy Measurement Validation of Differential Scanning Calorimeters Link
E967-08 Standard Test Method for Temperature Calibration of Differential Scanning Calorimeters and Differential Thermal Analyzers Link
E1356-08 Standard Test Method for Assignment of the Glass Transition Temperatures by Differential Scanning Calorimetry Link
D6604-00 Standard Practice for Glass Transition Temperatures of Hydrocarbon Resins by Differential Scanning Calorimetry Link
E928-08 Standard Test Method for Purity by Differential Scanning Calorimetry Link
E1269-11 Standard Test Method for Determining Specific Heat Capacity by Differential Scanning Calorimetry Link
E537-12 Standard Test Method for The Thermal Stability of Chemicals by Differential Scanning Calorimetry Link
E793-06 Standard Test Method for Enthalpies of Fusion and Crystallization by Differential Scanning Calorimetry Link
D3418-15 Standard Test Method for Transition Temperatures and Enthalpies of Fusion and Crystallization of Polymers by Differential Scanning Calorimetry Link
E2160-04 Standard Test Method for Heat of Reaction of Thermally Reactive Materials by Differential Scanning Calorimetry Link
D4591-07 Standard Test Method for Determining Temperatures and Heats of Transitions of Fluoropolymers by Differential Scanning Calorimetry Link
D3895-14 Standard Test Method for Oxidative-Induction Time of Polyolefins by Differential Scanning Calorimetry Link
E1582-14 Standard Practice for Calibration of Temperature Scale for Thermogravimetry Link
E2040-08 Standard Test Method for Mass Scale Calibration of Thermogravimetric Analyzers Link
E2402-11 Standard Test Method for Mass Loss and Residue Measurement Validation of Thermogravimetric Analyzers Link
E794-06 Standard Test Method for Melting and Crystallization Temperatures by Thermal Analysis Link
E1131-08 Standard Test Method for Compositional Analysis by Thermogravimetry Link
D6370-99 Standard Test Method for Rubber–Compositional Analysis by Thermogravimetry (TGA) Link
E1868-10 Standard Test Methods for Loss-On-Drying by Thermogravimetry Link
E2008-08e1 Standard Test Methods for Volatility Rate by Thermogravimetry Link
E2550-11 Standard Test Method for Thermal Stability by Thermogravimetry Link
D6382-99 Standard Practice for Dynamic Mechanical Analysis and Thermogravimetry of Roofing and Waterproofing Membrane Material Link
E1877-15 Standard Practice for Calculating Thermal Endurance of Materials from Thermogravimetric Decomposition Data Link
E2403-06 Standard Test Method for Sulfated Ash of Organic Materials by Thermogravimetry Link
E2043-99 Standard Test Method for Nonvolatile Matter of Agricultural Adjuvant Solutions by Thermogravimetry Link
D3850-12 Standard Test Method for Rapid Thermal Degradation of Solid Electrical Insulation Materials By Thermogravimetric Method (TGA) Link

 

ISO Number Title Website Link
11358 Plastics– Thermogravimetry (TG) of polymers Link
9924 Rubber and rubber products– Determination of the composition of vulcanizates and uncured compounds by thermogravimetry Link
21870 Rubber compounding ingredients– Carbon black– Determination of high-temperature loss on heating by thermogravimetry Link
11308 Nanotechnologies– Characterization of single-wall carbon nanotubes using thermogravimetric analysis Link
11357 Plastics– Differential scanning calorimetry (DSC) Link
18373 Rigid PVC pipes– Differential scanning calorimetry (DSC) method Link
15309 Implants for surgery– Differential scanning calorimetry of poly ether ether ketone (PEEK) polymers and compounds for use in implantable medical devices Link
16805 Binders for paints and varnishes– Determination of glass transition temperature Link
28343 Rubber compounding ingredients– Process oils– Determination of glass transition temperature by DSC Link
11409 Plastics– Phenolic resins– Determination of heats and temperatures of reaction by differential scanning calorimetry Link
22768 Rubber, raw– Determination of the glass transition temperature by differential scanning calorimetry (DSC) Link
14322 Plastics– Epoxy resins– Determination of degree of crosslinking of crosslinked epoxy resinsby differential scanning calorimetry Link